(1R-endo)-3-amino-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one hydrochloride

  • CAS：31638-54-7
  • purity：99%
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Details

Reliable Quality (1R-endo)-3-amino-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one hydrochloride 31638-54-7 Hot Sale with Chinese Manufacturer

  • Molecular Formula: C10H17 N O . Cl H
  • Molecular Weight: 203.712
  • Vapor Pressure: 0.00263mmHg at 25°C 
  • Melting Point: 234 - 236 °C 
  • Boiling Point: 282.1°Cat760mmHg 
  • Flash Point: 124.4°C 
  • PSA： 43.09000 
  • Density: g/cm3 
  • LogP: 2.84120 

(1R-endo)-3-amino-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one hydrochloride(Cas 31638-54-7) Usage

InChI:InChI=1/C10H17NO.ClH/c1-9(2)6-4-5-10(9,3)8(12)7(6)11;/h6-7H,4-5,11H2,1-3H3;1H/t6-,7+,10+;/m1./s1

31638-54-7 Relevant articles

Asymmetric reduction of α-keto aldoxime o -ethers

Bosiak, Mariusz J.,Pakulski, Marcin M.

experimental part, p. 316 - 324 (2011/03/18)

The catalytic asymmetric reduction of -k...

31638-54-7 Process route

3-endo-aminobornan-2-one
33162-63-9

3-endo-aminobornan-2-one

(1R,3S,4S)-(+)-3-amino-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one hydrochloride
31638-54-7

(1R,3S,4S)-(+)-3-amino-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one hydrochloride

Conditions
Conditions Yield
With hydrogenchloride; In diethyl ether;
(1R,3S,4S)-(+)-3-amino-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one hydrochloride
31638-54-7

(1R,3S,4S)-(+)-3-amino-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one hydrochloride

(1R,2R,3S,4S)-3-Amino-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-ol
29900-93-4

(1R,2R,3S,4S)-3-Amino-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-ol

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: sodium hydroxide / water / 0.02 h / 0 °C / pH 10
2: lithium aluminium tetrahydride / diethyl ether / 0 - 20 °C
With lithium aluminium tetrahydride; sodium hydroxide; In diethyl ether; water;

31638-54-7 Upstream products

  • 33162-63-9
    33162-63-9

    3-endo-aminobornan-2-one

31638-54-7 Downstream products

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    13747-75-6

    2β-Methyl-2α-isopropenyl-cyclohexanon

  • 29900-93-4
    29900-93-4

    (1R,2R,3S,4S)-3-Amino-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-ol

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